One Bath Acid Dyes – and “Textile Tattoos”

I have used one-bath acid dyes extensively in my own work, especially for cross-dyeing my handwoven fabrics that are constructed of both cotton and wool. The acid dyes attach only to the wool or other protein fiber. When combined with indigo, which attaches to both cellulose and protein fibers, very interesting combinations can be achieved. 

The “one-bath acid dyes” that Joy Boutrup and I discuss in The Art and Science of Natural Dyes include henna, madder, pomegranate, cochineal, lac, and rhubarb root. Since publishing the book, I have extended the palette with the addition of other dyes, mostly due to the help from Michel Garcia when he was here in my studio several years ago. 

Michel and I were discussing dyes that I might choose NOT to use because of their poor tolerance to light. Alkanet is one of those. A purple color is extracted from alkanet root by means of an alcohol extraction. The color is beautiful and enticing , but very fugitive. Michel indicated that the alcohol extraction does some damage to the dyestuff. 

The one-bath process extracts different dyes from the plant than from those that are obtained from using more traditional methods. While experimenting, we treated alkanet as a one bath acid dye (for protein fiber only) and a beautiful purplish brown color emerged that is quite fast to light. It’s a warm neutral color that I have not achieved using any other dye. 

Safflower petals are another dye source that he showed me can be used as a one-bath acid dye. A golden yellow is dyed onto wool or silk that is quite lightfast and requires no mordant. The safflower petals can still be used after the one-bath process to extract the traditional reds and pinks by altering the pH, though the red colors are still not fast to light. 

These discoveries energized my own work and as I went deeper,  I began noticing that many of the plant dyes that are used for the one-bath acid process have also been used as natural hair dyes: henna, madder, alkanet, dock, rhubarb root, cassia leaves (Cassia obovata, also referred to as “neutral” or “colorless” henna). These can all be used successfully for one-bath acid dyes and result in very lightfast colors. Dried Indigofera tinctoria leaves (“black henna”) are also used as a dye for hair and when combined with henna results in a very dark color. 

The application of henna as both a hair dye and as mehndi, (a temporary dye for the skin) is the same: finely ground plant material is mixed into a paste with water, acidified with lemon juice, and allowed to sit on the hair or skin for several hours. When the paste is washed away the color remains. These are considered non-permanent dyes for the skin and hair and may be repeated after the color fades. 

Acid dyes are very lightfast but are not as fast to washing. (This applies to both natural acid dyes and synthetic dyes.) If applied to the skin or hair, they will eventually be washed away.  BUT importantly, we don’t wash our woolen fabrics as aggressively or as often, thus the dyes are suitable for wool or silk textiles. 

I was curious to see if these dyes could be used for direct application to woolen fabrics. There is a Moroccan tradition of using finely ground henna leaf in this way on fabrics woven of wool and cotton. It is well documented in the book Die Farbe Henna / The Color of Henna Colour of Henna: Painted Textiles from Southern Morocco by Annette Korolnik-Andersch and Marcel Korolnik.

I made a paste of each of these dyes using finely ground plant material with a small amount of water. I acidified the paste with vinegar (citric acid would damage fabrics that contained cotton) and allowed it to sit overnight once applied to the textile. The colors are strong and clear, although some dyes spread more than others. They are not quite as deep as those dyed in a heated bath, though steaming the textiles will result in deeper colors. 

hand application of dye paste

I have observed that the freshness and quality of the dyes matter. Organic henna, used for hair and skin dye, resulted in a bright clear color while other henna powders that I have used produced duller colors. 

This approach has revealed to me one more way of understanding and using natural color and given me more opportunity to combining it with my own woven textiles. It has taught me more about plant categories, alternative applications, and the need to constantly be open to new ideas. 

What Size is YOUR Indigo Vat?

I now have, and am actively using, three 50 liter (15 gallon) indigo vats, in addition to a 100 liter (30 gallon) henna vat. 

I am loving the size of the 50 liter vat! The vessel is tall and narrow. It’s just the right shape for a vat, with a relatively reduced surface area, and a great size for studio immersion dyeing. I have been dyeing samples, skeins of yarn, my own shibori work, and even clothing in those vats. 

Like most dyers, I began with what I then thought was a “large” 5 gallon vat. That is still the most practical size for teaching workshops and I am guessing that it’s the size/shape that many dyers start with – and most stay with. 

But, I don’t think it’s the best for studio work. IT’S TOO SMALL!  When working with natural indigo vats, whether they are fermentation vats or quick reduction vats, there is going to be a lot of ‘sludge” at the bottom of the vat. With some vats this can be up to 1/3, or more, of the total depth. If you keep the textiles above that sludge , it doesn’t leave much room for dyeing. I am afraid that many dyers might tend to let their textiles dip into that “wasteland” at the bottom, exposing the fibers to concentrated lime or plant material. As a result, the dyeing is not as good as it could be. 

A 50 liter/15 gallon liter vat is a much greater commitment than an 18 liter/ 5 gallon bucket, both in terms of financial investment and engagement.  Yet, it is so much more useful and the dyeing is so much better! It’s also harder to just “give up” on a larger vat. You get better at maintaining and problem solving.

This is the vessel that I use. It’s a hard, durable plastic. I place it on a wheeled dolly. Otherwise it’s too difficult to move. A heavy duty plant caddy works just fine. 

Sometimes I suspend samples and other small pieces from the top, using stainless hooks and wooden rods. 

I have experimented with several types of baskets, nets, etc. to hold my larger textiles and keep them away from the bottom of the vat. I have finally settled on using a large, mesh laundry bag. It fits the vessel nicely, is flexible, re-usable, completely contains the textiles, and prevents things from getting lost in the bottom. 

As I experiment with the fermentation vats, it becomes necessary to do a lot of dyeing. I am working on a long-term woven series, but regular dyeing has become increasingly important with my fermentation vats – and more possible, now that I am staying home.

I’ve taken some of my white or light colored clothing (too impractical to wear in the studio) and turned them into indigo dyed “dyeing clothes”. It took some courage to put a large linen tunic in the vat but I’ve been surprised at the even dyeing of even these larger,  constructed  pieces. I always do at least 3 long dips into the vat, which will assure that the dye “evens out”. I would never have attempted dyeing clothing in a 5 gallon vat.

Maintaining a good dyeing temperature is important, especially with the fermented vats. I have successfully used a band-type pail warmer and plugged it into a digital temperature controller. This has been keeping the vats at a regular temperature in my unheated studio. 

AND if you are going to make wood ash lye for a fermentation vat, this is the time of year to connect with friends who are burning wood. You will want to identify someone who burns only hard wood in an efficient wood stove. That will result in the best ash for making lye.